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Commercial cereals vary considerably in composition, both in their formulation and the ingredients added to enrich these products. Sodium is the predominant cation in breakfast cereals, at levels reaching 8mg/g. Potassium and calcium also vary, particularly in wheat-based products and those enriched with milk products or calcium salts.
This method for the measurement of sodium and potassium in silicate rocks uses a borate fusion technique.
A number of methods have been reported for the measurement of calcium in biological materials by flame photometry or titration. This method employs trichloroacetic acid (TCA) to precipitate the proteins and has been found to be adequate to extract all of the calcium from tissue samples. Sodium, potassium and phosphate caused no significant interference and calcium concentration in the range of 0 to 2 µg/ml is readily determined.